如何分析阿卡波糖?/ Acarbose Analysis

發文者: 達哥

 

阿卡波糖(Acarbose)為近年興起的降血糖藥物,因不會對人體有抗藥性的產生而被廣為使用。

問題

如何分析阿卡波糖?

使用條件

移動相: ACN/ Phosphate Buffer (600 mg Monopotassium Phosphate and

            279 mg Sodium hydrogen phosphate, anhydrous in 1000 mL

            volumetric flask, add water to 1 L mark) 80/20

 

流速:  2.0 mL/min

溫度: 35℃

偵測器 : UV 210 nm

注射體積 : 50 uL

管柱: Hypersil APS-2, 5 um 4.0 X 250 mm

回應

Answer:原廠提供建議分析方法

其他說明

Thermo Fisher 是液相色譜柱技術的領導者,包括矽,聚合物和多孔石墨碳的製造,以及鍵合相的生產和層析管柱的製造。在此陳列最新最全面的LC,HPLC和UHPLC的層析管柱。



 

Question

Acarbose Analysis

Condition

Mobile Phase : ACN/ Phosphate Buffer (600 mg Monopotassium Phosphate and 279 mg Sodium hydrogen phosphate, anhydrous in 1000 mL volumetric flask, add water to 1 L mark) 80/20

 

Flow rate : 2.0 mL/min,

Column temperature: 35℃,

Detection wavelength : 210 nm

Injection volume : 50 uL

Column: PN:30705-254030, HypersilAPS-2, 5 um 4.0 X 250 mm

Answer

Thermo Fisher suggest analysis method.

Other instructions

Thermo Fisher Scientific is the world leader in serving science, with revenues of more than $20 billion and approximately 70,000 employees globally. Our mission is to enable our customers to make the world healthier, cleaner and safer. We help our customers accelerate life sciences research, solve complex analytical challenges, improve patient diagnostics, deliver medicines to market and increase laboratory productivity. Through our premier brands – Thermo Scientific, Applied Biosystems, Invitrogen, Fisher Scientific and Unity Lab Services – we offer an unmatched combination of innovative technologies, purchasing convenience and comprehensive services.

 

 

Part Number

品名

30705-254030

Hypersil APS-2, 5 um 4.0 X 250 mm

 

參考圖譜

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Part Number

品名

30705-254030

Hypersil APS-2, 5 um 4.0 X 250 mm


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